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1 article(s) from Meyer, Annemarie

Syntheses and properties of thienyl-substituted dithienophenazines

Annemarie Meyer,
Eva Sigmund,
Friedhelm Luppertz,
Gregor Schnakenburg,
Immanuel Gadaczek,
Thomas Bredow,
Stefan-S. Jester and
Sigurd Höger

Beilstein J. Org. Chem. 2010, 6, 1180–1187, doi:10.3762/bjoc.6.135

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Scheme 1: Synthesis of 4. a) 1) EtLi, Et₂O, −78 °C, 1 h; 2) (COOMe)₂, Et₂O, −78 °C, 2 h, 33%; b) FeCl₃, MeNO₂...

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Scheme 2: Synthesis of 8. a) Pd(PPh₃)₄, Na₂CO₃, toluene, EtOH, H₂O, reflux, 87%; b) oxalyl chloride, 1,2-dich...

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Scheme 3: Preparation of phenazine isomers. a) AcOH, 50 °C, 2 h, 93% (10a), 53% (10b). b) AcOH, 50 °C, 2 h, 6...

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Scheme 4: Suzuki–Miyaura reactions with 10a/10b. a) Pd(PPh₃)₄, Na₂CO₃, toluene, EtOH, H₂O, reflux, 23% (12a),...

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Scheme 5: Suzuki–Miyaura reactions with 11a/11b. a) Pd(PPh₃)₄, Na₂CO₃, toluene, EtOH, H₂O, reflux, 50% (16), ...

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Figure 1: a) Absorption (solid lines) and emission (dotted lines) spectra of compounds 12a (blue), 13 (red), ...

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Figure 2: Calculated absorption spectra of (a) 19, (b) 20, (c) 12a, (d) 13 with R=CH₃, (e) 16 and (f) 17a. In...

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Figure 3: Self-assembled monolayer of 12b on HOPG. a) STM image (V_S = −0.8 V, I_t = 80 pA, image size 25.0 × 2...

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Published 13 Dec 2010

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